王君,栾玲玉,张继斌,王望舒,武吉伟,郭风.食品包装用 PVC 中 3 种增塑剂的残留及特定条件下的迁移规律[J].包装工程,2013,34(1):29-33.
WANG Jun,LUAN Ling-yu,ZHANG Ji-bin,WANG Wang-shu,WU Ji-wei,GUO Feng.Study on Residual and Migration of Three Plasticizers in Food Contact PVC Packaging under Specified Conditions[J].Packaging Engineering,2013,34(1):29-33.
食品包装用 PVC 中 3 种增塑剂的残留及特定条件下的迁移规律
Study on Residual and Migration of Three Plasticizers in Food Contact PVC Packaging under Specified Conditions
投稿时间:2012-10-25  修订日期:2013-01-10
DOI:
中文关键词:  增塑剂  迁移  残留  食品包装  食品模拟液
英文关键词:plasticizer  migration  residue  food packaging  food stimulant
基金项目:山东省质量技术监督局科研项目(2010KYZ03)
作者单位
王君 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; 
栾玲玉 山东省分析测试中心, 济南 250014 
张继斌 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; 
王望舒 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; 
武吉伟 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; 
郭风 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; 
AuthorInstitution
WANG Jun 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; 
LUAN Ling-yu Shandong Analysis and Test Center, Jinan 250014, China 
ZHANG Ji-bin 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; 
WANG Wang-shu 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; 
WU Ji-wei 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; 
GUO Feng 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; 
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中文摘要:
      采用气相色谱-质谱(GC-MS)法测定了食品包装用 PVC 中 DBP,DEHP 和 DEHA 3 种增塑剂的残留,然后结合凝胶渗透色谱(GPC)技术研究了高温下 3 种增塑剂在脂类食品(模拟液)中的迁℃规律。 结果表明,PVC食品包装中均不同程度地有 3 种增塑剂残留,残留的增塑剂在高温(80,100 ℃ )条件下,极易快速迁℃至脂类食品(模拟液)中,甚至超过欧盟的限量标准(1. 5 mg / kg),且迁℃量随时间延长而增加。
英文摘要:
      3 kinds of plasticizer DBP, DEHP, and DEHA in food contact PVC packaging were determined using GCMS method. The migration of the plasticizers into oil-type foodstuff simulants at high temperature was studied by combining GC-MS and gel permeation chromatography (GPC). The results indicated that 3 kinds of plasticizer exist in the food contact PVC with different contents; the existing plasticizers can easily migrate into oil-type food simulants quickly under high temperature (80 ℃ , 100 ℃ ), and the amount of migration exceeds the required limited quantity of 1. 5 mg / kg in EU; moreover, the migration quantity increases with time extending.
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