王君,栾玲玉,张继斌,王望舒,武吉伟,郭风.食品包装用 PVC 中 3 种增塑剂的残留及特定条件下的迁移规律[J].包装工程,2013,34(1):29-33.
WANG Jun,LUAN Ling-yu,ZHANG Ji-bin,WANG Wang-shu,WU Ji-wei,GUO Feng.Study on Residual and Migration of Three Plasticizers in Food Contact PVC Packaging under Specified Conditions[J].Packaging Engineering,2013,34(1):29-33. |
| 食品包装用 PVC 中 3 种增塑剂的残留及特定条件下的迁移规律 |
| Study on Residual and Migration of Three Plasticizers in Food Contact PVC Packaging under Specified Conditions |
| 投稿时间：2012-10-25 修订日期：2013-01-10 |
| DOI： |
| 中文关键词: 增塑剂 迁移 残留 食品包装 食品模拟液 |
| 英文关键词:plasticizer migration residue food packaging food stimulant |
| 基金项目:山东省质量技术监督局科研项目(2010KYZ03) |
| 作者 | 单位 |
| 王君 | 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; |
| 栾玲玉 | 山东省分析测试中心, 济南 250014 |
| 张继斌 | 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; |
| 王望舒 | 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; |
| 武吉伟 | 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; |
| 郭风 | 1. 山东省产品质量监督检验研究院, 济南 250103; 2. 山东省材料化学安全检测技术重点实验室, 济南250103; |
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| Author | Institution |
| WANG Jun | 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; |
| LUAN Ling-yu | Shandong Analysis and Test Center, Jinan 250014, China |
| ZHANG Ji-bin | 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; |
| WANG Wang-shu | 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; |
| WU Ji-wei | 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; |
| GUO Feng | 1. Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China; 2. Shandong Provincial Key Laboratory of Test Technology for Material Chemical Safety, Jinan 250103, China; |
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| 中文摘要: |
| 采用气相色谱-质谱(GC-MS)法测定了食品包装用 PVC 中 DBP,DEHP 和 DEHA 3 种增塑剂的残留,然后结合凝胶渗透色谱(GPC)技术研究了高温下 3 种增塑剂在脂类食品(模拟液)中的迁℃规律。 结果表明,PVC食品包装中均不同程度地有 3 种增塑剂残留,残留的增塑剂在高温(80,100 ℃ )条件下,极易快速迁℃至脂类食品(模拟液)中,甚至超过欧盟的限量标准(1. 5 mg / kg),且迁℃量随时间延长而增加。 |
| 英文摘要: |
| 3 kinds of plasticizer DBP, DEHP, and DEHA in food contact PVC packaging were determined using GCMS method. The migration of the plasticizers into oil-type foodstuff simulants at high temperature was studied by combining GC-MS and gel permeation chromatography (GPC). The results indicated that 3 kinds of plasticizer exist in the food contact PVC with different contents; the existing plasticizers can easily migrate into oil-type food simulants quickly under high temperature (80 ℃ , 100 ℃ ), and the amount of migration exceeds the required limited quantity of 1. 5 mg / kg in EU; moreover, the migration quantity increases with time extending. |
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