潘曦,杨俊鹏,王昊,何昀潞,肜霖,王磊.基于SPME-GC-MS分析卷烟包装材料挥发性气体的研究[J].包装工程,2021,42(17):118-124.
PAN Xi,YANG Jun-peng,WANG Hao,HE Yun-lu,RONG Lin,WANG Lei.Analysis of Volatile Gas in Cigarette Packaging Materials Based on SPME-GC-MS[J].Packaging Engineering,2021,42(17):118-124.
基于SPME-GC-MS分析卷烟包装材料挥发性气体的研究
Analysis of Volatile Gas in Cigarette Packaging Materials Based on SPME-GC-MS
投稿时间:2020-10-22  
DOI:10.19554/j.cnki.1001-3563.2021.17.015
中文关键词:  卷烟包装材料  挥发性气体  气相色谱-质谱联用  固相微萃取
英文关键词:cigarette packaging materials  volatile gases  gas chromatography-mass spectrometry  solid phase microextraction
基金项目:绿色轻工材料湖北省重点实验室开放基金(0136-1200951)
作者单位
潘曦 湖北中烟工业有限责任公司,武汉 430040 
杨俊鹏 湖北中烟工业有限责任公司,武汉 430040 
王昊 湖北中烟工业有限责任公司,武汉 430040 
何昀潞 湖北中烟工业有限责任公司,武汉 430040 
肜霖 湖北中烟工业有限责任公司,武汉 430040 
王磊 湖北工业大学 绿色轻工材料湖北省重点实验室,武汉 430068 
AuthorInstitution
PAN Xi China Tobacco Hubei Industrial LLC, Wuhan 430040, China 
YANG Jun-peng China Tobacco Hubei Industrial LLC, Wuhan 430040, China 
WANG Hao China Tobacco Hubei Industrial LLC, Wuhan 430040, China 
HE Yun-lu China Tobacco Hubei Industrial LLC, Wuhan 430040, China 
RONG Lin China Tobacco Hubei Industrial LLC, Wuhan 430040, China 
WANG Lei Hubei Provincial Key Laboratory of Green Materials for Light Industry, Hubei University of Technology, Wuhan 430068, China 
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中文摘要:
      目的 建立一种高效且准确的分析测试方法,快速检测卷烟包装材料中挥发性气体的类别和含量。方法 基于气相色谱-质谱联用(GC-MS),比较传统顶空-气相色谱-质谱联用(HS-GC-MS)和固相微萃取-气相色谱-质谱联用(SPME-GC-MS)的检测效果,并对SPME-GC-MS检测的各项参数进行优化。结果 确定了SPME-GC-MS定性、定量分析卷烟材料气味的最优分析条件,并对印刷工艺较为复杂的盒包卷烟包装材料进行了高效、准确的检测。结论 建立的SPME-GC-MS方法可以对盒包卷烟包装材料挥发性气体的异味进行定性和定量分析,为盒包材料的品质评价和印刷过程中异味的检测提供了新的策略。
英文摘要:
      To establish an efficient and accurate analytical test method for quick detection of the type and content of volatile gases in cigarette packaging materials. With the help of gas chromatography-mass spectrometry (GC-MS), the detection performance of traditional headspace-gas chromatography-mass spectrometry (HS-GC-MS) and solid phase microextraction-gas chromatography-mass spectrometry (SPME-GC-MS) were compared respectively, and the parameters of SPME-GC-MS were optimized. The optimal analysis conditions for qualitative and quantitative analysis of the odor of cigarette materials by SPME-GC-MS were determined, and the packaging materials of cigarette packs with complicated printing processes were detected efficiently and accurately. The SPME-GC-MS method established in this paper can be used to qualitatively and quantitatively analyze the volatile odors of cigarette packaging materials and provides a new strategy for the quality evaluation of the packaging materials and the odor detection during the printing process.
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